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Inline Refractometer for Process Concentration & Brix Measurement

Inline Refractometer for Process Concentration and Brix Measurement

An inline refractometer is a real-time concentration measurement instrument based on the principle of optical refraction. When light passes from one medium into another, its path is deflected; this angle of deflection is directly related to the content of soluble solids in the liquid.

The Inline Refractometer measures and displays parameters required by users, such as concentration (%) and Brix. It can be directly installed on pipelines or reactors to enable real-time, continuous, and online monitoring of liquid concentration during the production process. Compared to traditional manual sampling methods, the inline refractometer completely eliminates sampling delays and human error.

  • Real-time, rapid detection ensures production quality and facilitates maintenance.
  • High precision, unique algorithms, and automatic temperature compensation.
  • Customizable installation methods and cleaning options.
  • Configurable interfaces include 4–20 mA, RS-485, RS-232, and USB; optional modules for alarm, cleaning, and switch signal outputs are also available.

Benefits

Measuring PrincipleCritical angle of total internal reflection. Readings are not affected by bubbles, suspended solids or sample color.
Robust ConstructionSapphire prism with 316L stainless steel housing. Resists corrosion and is rated to 1.5 MPa.
Temperature CompensationA built-in sensor tracks process temperature in real time and automatically compensates readings to a reference temperature.
Low MaintenanceModular design with no wearing parts, so it needs very little routine service.
  • Flexible Installation: Adapts to complex environments such as pipelines and tanks, saving installation time and costs.
  • Stable Measurement: Advanced technology ensures measurements are not affected by medium characteristics (bubbles, color, turbidity, etc.) or operating conditions (pressure, flow rate, etc.), providing stable and accurate data.
  • Convenient Calibration: Probes are rigorously calibrated before shipment and feature built-in temperature compensation, making the complete system ready for immediate use upon delivery.
  • Smart Customization: Equipped with a built-in concentration data processing system, users can build data models on-site and customize parameters to improve testing accuracy.
  • Self-Diagnostic Maintenance: Features probe status self-diagnosis to quickly pinpoint faults and minimize downtime.
  • On-Site Calibration: Supports refractive index (RI) calibration and adjustment, allowing for real-time correction of detection errors.
  • Intelligent and Durable: Utilizes an intelligent chip, requires no reagents or consumables, has low power consumption, and features a probe light source with a lifespan of up to 100,000 hours.
  • One-Stop Solution: Leveraging these performance advantages, it provides a one-stop solution for industrial testing, enhancing production efficiency and ensuring product quality control.

Technical Specifications

ModelCRN50CRN52CRN56
Measured ParametersRefractive index, temperature, concentration, Brix (or other scales)
Displayed ParametersRefractive index (nD), Brix (temperature-compensated per sucrose), concentration (Conc), temperature (°C)
Data ProcessingProbe status diagnostics, RI calibration and adjustment, user self-modeling, multi-point temperature compensation, concentration curve correction
Concentration Range0.0–90% Brix0.0–100% Brix
Refractive Index Range1.33299–1.517821.33299–1.57041
Process Temperature0–60 °C0–70 °C-10–100 °C
Cleaning Temperature-30–120 °C, supports CIP (clean-in-place) and SIP (sterilize-in-place)
Resolution0.01%; refractive index 0.00001; temperature 0.1 °C
Accuracy±0.1%; refractive index 0.0001; temperature 0.5 °C
Process ConnectionCompact clamp (optional flange: DN25 / DN50 / DN65 / DN80)
Wetted MaterialsSS316L + high-strength optical glassSS316L + sapphire (optional: PTFE, Hastelloy, titanium, tantalum)
Power SupplyStandard: 24 VDC; optional: 100–240 VAC, 50/60 Hz, 30 VA
Cable LengthStandard 2 m, extendable up to 200 m
Display1.4-inch on-board display
Signal Output4–20 mA / RS485 / RS232 / USB
Ingress ProtectionWetted part IP68
Pressure Rating≤1.5 MPa
Explosion ProtectionEx ia IIC T6 Ga
Net Weight≈1.0 kg
Cleaning OptionsCRN5-C1 ultrasonic cleaning assembly; CRN5-C2 high-pressure flushing assembly
Installation OptionsSmall-bore pipe adapter, tee / cross (with sight window), sanitary adapter, etc., customized to installation conditions

Optional Accessories

Dimensional Drawing of Inline Refractometer

Compact clamp-style mount; available in sizes: DN25/DN50/DN65/DN80.

Total length: 121.45 mm; distance from clamp face to rear: 114.45 mm;
Probe extension length: 26.15 mm; finned housing length: 63.50 mm;
Clamp outer diameter: Φ77.50 mm; probe diameter: Φ31.00 mm (with options for Φ56.00 / Φ48.00 mm);
Electrical connection: GX20 12-pin aviation connector; display window height: 14.86 mm.

Inline Refractometer Working Principle

1. Light Propagation and the Phenomenon of the Critical Angle

Measurements with an inline refractometer begin with the propagation of light. Light emitted by a high-brightness LED is guided through a low-loss optical fiber and introduced from a specific side of the prism. Inside the prism, the light follows a carefully designed reflection path until it reaches the interface between the prism and the liquid being measured. At this critical interface, the propagation behavior of light differs significantly due to the varying refractive indices of the two liquids.

According to optical principles, when light travels from a denser medium to a less dense medium, total internal reflection occurs at a specific angle of incidence.

In an online refractometer, some light rays satisfy the conditions for total internal reflection and are completely reflected to the other side of the prism. Furthermore, the position of the total internal reflection light changes as the critical angle varies, since the critical angle is closely related to the liquid’s refractive index; even slight changes in the liquid’s refractive index directly cause corresponding changes in the critical angle.

Inline refractometer working principle: critical angle of total reflection detected by a CCD array

2. Optical-to-Electrical Conversion for Concentration Measurement

To accurately capture changes in the position of the total reflection light, the online refractometer employs a linear array CCD. It precisely detects the position of the light-dark boundary of the total reflection light, with each specific position uniquely corresponding to a specific refractive index value.

It is worth noting that there is a clear correlation between the solution concentration and the position of the light-dark boundary: as the solution concentration increases, the light-dark boundary shifts further to the left.

The online refractometer uses optical methods to measure the critical angle of the solution and employs a hybrid analog-digital principle to determine the solution’s concentration. A light source inside the sensor emits light at different angles toward the prism and the interface with the solution being measured.

Due to the different angles of incidence, the light behaves differently at the interface: some light is totally reflected, some is partially reflected, and most is refracted into the solution being measured, thereby creating a unique optical image consisting of bright and dark regions at the interface.

The angle of incidence corresponding to the boundary line between the dark and bright zones is defined as the “critical angle.” Changes in the critical angle directly alter the brightness-to-darkness ratio detected by the CCD sensor; this ratio is, in fact, a function of the refractive index.

Given the stable correlation between solution concentration and refractive index, the solution’s concentration can be accurately determined by precisely measuring the critical angle.

3. Signal Processing and Temperature Compensation

During signal detection and processing, the online refractometer uses a digital CCD (charge-coupled device) to meticulously detect the optical image and the boundary shadow line. It converts complex image information point by point into electrical signals that are easy to process. Through precise analysis of these electrical signals, the exact position of the boundary shadow line is determined, thereby accurately measuring the refractive index nD.

At the same time, the probe incorporates a high-precision temperature sensor that measures the temperature of the medium at the interface in real time.

After acquiring data on the refractive index nD and temperature T, the transmitter automatically performs temperature compensation based on a preset algorithm, thereby precisely calculating and intuitively displaying the concentration value of the liquid.

The preliminarily processed electrical signals undergo further gain amplification and are then converted into various practical parameters, such as mass concentration, solids content, Brix, density, and refractive index. These parameters are not only clearly displayed locally on the instrument but can also be transmitted over long distances via remote transmission technology, providing robust support for real-time monitoring and automated control in industrial production processes.

Featured Application

Thanks to its high accuracy, real-time performance, and stability, the Inline Refractometer has found widespread application in numerous fields.

In the food and beverage industry, it can be used to monitor concentration during the production of products such as sucrose, fruit puree, jelly, soft drinks, fructose, milk, beer, glucose, fruit juice, and bone broth, ensuring stable and consistent product quality.

In the chemical industry, it is suitable for concentration testing of various chemical raw materials and products, such as sulfuric acid, hydrochloric acid, phosphoric acid, sodium hydroxide, ammonia water, urea, surfactants, ethylene glycol, hydrogen peroxide, sodium hypochlorite, methanol, and ethanol, thereby ensuring the safe and efficient operation of chemical production.

In other industries, such as the concentration measurement of cutting fluids, coolants, DMF, DMAC, PVOH, traditional Chinese medicine concentrates, emulsions, slurries, polyurethanes, alcohol extracts, sodium carbonate, glycerin, gelatin, and collagen peptides, it also plays a vital role in helping various industries improve production efficiency and product quality.

With their advanced measurement principles and wide range of applications, online refractometers have become indispensable tools in modern industrial production and scientific research.

Inline Refractometers

Installation Guide

The inline refractometer reads only the liquid touching the prism window. A good installation keeps that window fully covered by a moving, bubble-free sample.

Mounting Options

Mounting Position

The sample must fill the pipe and cover the prism surface. Positions ① to ③ are recommended. Positions ④ and ⑤ are not allowed.

Recommended and incorrect mounting positions for an inline refractometer

Never install the probe with the prism facing down, whether on a pipe or a tank. On a horizontal line, gas collects at the top of the pipe. In a vertical line with downward flow, the pipe may not run full.

Inline refractometer installation on large pipes, 2-inch pipes and vessel walls

On large and medium pipes, insert the probe at an angle with the tip facing the flow. On 2-inch and smaller lines, use a flanged spool piece so the tip sits in the flow path. On vessels, mount through the wall at a point where the liquid is moving.

Before You Install

Installation Notes

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